Methyl 6-bromo-7-methoxy-1,3-benzodioxole-5-carboxylate

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Methyl 6-bromo-7-meth­oxy-1,3-benzodioxole-5-carboxyl­ate

The non-H atoms of the title compound, C(10)H(9)BrO(5), are essentially coplanar, with the exception of the ester group [the O=C-O-C torsion angle is -143.4 (3)°].

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Methyl 5-bromo-6-methyl­picolinate

The title compound, C(8)H(8)BrNO(2), does not show any significant inter-molecular π-π or C-H⋯π inter-actions in the crystal packing except for one weak Br⋯Br [3.715 (1) Å] inter-action.

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Crystal structure of methyl 5-acetamido-2-t-butyl-2-methyl-1,3-benzodioxole-4-carboxylate.

1,3-benzodioxle-4-carboxylic acid] was designed as a novel class of chiral fluorometric agents.1 The chiral agent and the analogues have been conveniently applied to enantiomer analyses of various bio-molecules using HPLC and circular dichroism.2 We recently extended the molecular design of (S)TBMB carboxylic acid to chiral nitrobenzoic acids possessing the asymmetric 1,3-benzodioxole.3 The chi...

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6-Meth­oxy­meth­oxy-7-trifluoro­methyl-1,3-benzodioxole-5-carbaldehyde

The title compound, C(11)H(9)F(3)O(5), crystallizes with three mol-ecules in the asymmetric unit. One -CF(3) group is disordered by rotation, with the F atoms split over two sets of sites with occupancies which converged to 0.888 (6) and 0.112 (6). Weak π-π inter-actions are observed between adjacent benzene rings [the shortest centroid-centroid distance is 3.8858 (4) Å], resulting in the forma...

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(5S,6R)-6-Bromo-6-methyl-5-phenyl-3,4,5,6-tetra­hydro-2H-cyclo­penta­[b]pyran-7-one

The title compound, C(15)H(15)BrO(2), was synthesized by a Brønsted acid-catalysed domino electrocyclization-halogenation reaction. The five-membered ring is essentially planar (r.m.s. deviation 0.006 Å) and forms a dihedral angle of 72.7 (3)° with the attached phenyl ring. The six-membered heterocycle adopts a half-chair conformation. The crystal packing is stabilized by a C-H⋯O contact.

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ژورنال

عنوان ژورنال: Acta Crystallographica Section E Structure Reports Online

سال: 2008

ISSN: 1600-5368

DOI: 10.1107/s1600536808019399